Looks like everyone's riding on a single reference to this 1968 paper that makes the 3000 BCE claim: https://eurekamag.com/research/014/507/014507621.php
[edit] here is a link to the original NYT article from June of 2020 https://archive.is/ZuSyc
https://www.wired.com/story/the-teeny-tiny-scientific-screwu...
Archive link for research and education. https://archive.is/z14Ia