Let's take water as an example. Say you've got a supply of all the atoms you need and a way to place them precisely enough to reliably get water rather than a mix of hydrogen peroxide and hydrogen gas.
When the atoms combine, they release as much energy as burning hydrogen in oxygen. Equivalent problems for virtually everything.
I'm not sure if it's provably impossible, but AFAIK there is no known way to cool this down fast enough to even be stable for the duration of the TV show's materialisation sequence.